遷移元素分析のための試料調製<br>Sample Preparation for Trace Element Analysis (Comprehensive Analytical Chemistry)

遷移元素分析のための試料調製
Sample Preparation for Trace Element Analysis (Comprehensive Analytical Chemistry)

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  • 製本 Hardcover:ハードカバー版／ページ数 1446 p.
  • 言語 ENG
  • 商品コード 9780444511010
  • DDC分類 543.19

基本説明

Contetns: Digestion and Extraction Approaches(Wet digestion methods; Dry ashing etc.); Matrices(Sample prepatation for crude oil, petroleum products and polymers...); Trace Element Speciation(Smaple preparation for metal-based drugs etc.).

Full Description


Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. "Sample Preparation for Trace Element Analysis" is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation. This is the first title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. All the 39 chapters are authored by international leaders of their fields.

Contents

(Selected) Sampling and Sample Preservation for Trace Element Analysis Calibration approaches for trace element determination Detection Methods for the Quantitation of Trace Elements Dry ashing Fusion and fluxes Accelerated Solvent Extraction of Organometallic and Inorganic Compounds Solid Phase Microextraction as a Tool for Trace Element determination Chelation solvent extraction for separation of metal ions Sample preparation of geological samples, soils and sediments Aerosol sampling and sample preparation for elemental analysis Sample preparation for arsenic speciation Sample preparation for metal-based drugs